Interlaboratory comparison of measurements of acid-volatile sulfide and simultaneously extracted nickel in spiked sediments

Environ Toxicol Chem. 2011 Jun;30(6):1306-9. doi: 10.1002/etc.506. Epub 2011 Mar 31.

Abstract

An interlaboratory comparison of acid-volatile sulfide (AVS) and simultaneously extracted nickel (SEM_Ni) measurements of sediments was conducted among five independent laboratories. Relative standard deviations for the seven test samples ranged from 5.6 to 71% (mean = 25%) for AVS and from 5.5 to 15% (mean = 10%) for SEM_Ni. These results are in stark contrast to a recently published study that indicated AVS and SEM analyses were highly variable among laboratories.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Environmental Monitoring / methods
  • Geologic Sediments / chemistry*
  • Laboratories
  • Nickel / analysis*
  • Sulfides / analysis*
  • Water Pollutants, Chemical / analysis*

Substances

  • Sulfides
  • Water Pollutants, Chemical
  • Nickel