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Clinical utility of simultaneous quantitation of 25-hydroxyvitamin D and 24,25-dihydroxyvitamin D by LC-MS/MS involving derivatization with DMEQ-TAD.
Kaufmann M, Gallagher JC, Peacock M, Schlingmann KP, Konrad M, DeLuca HF, Sigueiro R, Lopez B, Mourino A, Maestro M, St-Arnaud R, Finkelstein JS, Cooper DP, Jones G. Kaufmann M, et al. Among authors: sigueiro r. J Clin Endocrinol Metab. 2014 Jul;99(7):2567-74. doi: 10.1210/jc.2013-4388. Epub 2014 Mar 26. J Clin Endocrinol Metab. 2014. PMID: 24670084 Free PMC article.
Stereoselective synthesis of 25S,26-dihydroxyvitamin D3.
Sigüeiro R, González-Berdullas P, Loureiro J, Mouriño A, Maestro MA. Sigüeiro R, et al. J Steroid Biochem Mol Biol. 2018 Mar;177:247-249. doi: 10.1016/j.jsbmb.2017.07.016. Epub 2017 Jul 18. J Steroid Biochem Mol Biol. 2018. PMID: 28732680
Synthesis of 28,28,28-trideutero-25-hydroxydihydrotachysterol2.
Sigüeiro R, Loureiro J, González-Berdullas P, Mouriño A, Maestro MA. Sigüeiro R, et al. J Steroid Biochem Mol Biol. 2019 Jan;185:248-250. doi: 10.1016/j.jsbmb.2018.09.014. Epub 2018 Sep 19. J Steroid Biochem Mol Biol. 2019. PMID: 30244048
Synthesis of nonadeuterated 1α,25-dihydroxyvitamin D2.
Sigüeiro R, Álvarez A, Otero R, López-Pérez B, Carballa D, Regueira T, González-Berdullas P, Seoane S, Pérez-Fernández R, Mouriño A, Maestro MA. Sigüeiro R, et al. J Steroid Biochem Mol Biol. 2014 Oct;144 Pt A:204-6. doi: 10.1016/j.jsbmb.2013.10.025. Epub 2013 Nov 1. J Steroid Biochem Mol Biol. 2014. PMID: 24189543 Review.
23 results